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Supervised by Ministry of Industry and Information Technology of The People's Republic of China Sponsored by Harbin Institute of Technology Editor-in-chief Yu Zhou ISSNISSN 1005-9113 CNCN 23-1378/T

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Spreading and Curing Behaviors of a Thermosetting Droplet-Silicone on a Heated Surface
Author NameAffiliationPostcode
Xingjian Yu School of Energy and Power Engineering, Huazhong University of Science and Technology, Wuhan 430074, China 430074
Run Hu School of Energy and Power Engineering, Huazhong University of Science and Technology, Wuhan 430074, China 430074
Liliang Zhou School of Energy and Power Engineering, Huazhong University of Science and Technology, Wuhan 430074, China 430074
Han Wu School of Energy and Power Engineering, Huazhong University of Science and Technology, Wuhan 430074, China 430074
Xiaobing Luo* School of Energy and Power Engineering, Huazhong University of Science and Technology, Wuhan 430074, China 430074
Abstract:
Thermosetting materials are widely used as encapsulation in the electrical packaging to protect the core electronic components from external force, moisture, dust, and other factors. However, the spreading and curing behaviors of such kind of fluid on a heated surface have been rarely explored. In this study, we experimentally and numerically investigated the spreading and curing behaviors of the silicone (OE6550 A/B, which is widely used in the light-emitting diode packaging) droplet with diameter of ~2.2 mm on a heated surface with temperature ranging from 25 °C to 250 °C. For the experiments, we established a setup with high-speed camera and heating unit to capture the fast spreading process of the silicone droplet on the heated surface. For the numerical simulation, we built a viscosity model of the silicone by using the N. Kiuna’s model and combined the viscosity model with the Volume of Fluid (VOF) model by the User Defined Function (UDF) method. The results show that the surface temperature significantly affected the spreading behaviors of the silicone droplet since it determines the temperature and viscosity distribution inside the droplet. For surface temperature varied from 25 °C to 250 °C, the final contact radius changed from ~2.95 mm to ~1.78 mm and the total spreading time changed from the ~511 s to ~0.15 s. By further analyzing the viscosity evolution of the droplet, we found that the decreasing of the total spreading time was caused by the decrease of the viscosity under high surface temperature at initial spreading stage, while the reduction of the final contact radius was caused by the curing of the precursor film. This study supplies a strategy to tuning the spreading and curing behavior of silicone by imposing high surface temperature, which is of great importance to the electronic packaging.
Key words:  thermosetting material  silicone  surface temperature  spreading and curing
DOI:10.11916/j.issn.1005-9113.2019018
Clc Number:O35
Fund:

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