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| Abstract: |
| A fourth generation single crystal (SC) nickel based cast superalloy DD15 with 1%Ru, 3%Ru, 5%Ru was prepared using vacuum induction single crystal furnace in order to optimize the properties and cost of DD15 alloy. The exposure experiment of three alloys was conducted at 1100 ℃ for 1000 h. The stress rupture properties tests were performed at 1100 ℃ temperature and 137 MPa pressure. The composition optimization of Ru element in DD15 alloy had been studied. It was found that the alloys with different Ru contents all consist of cuboidal γ′ phase embedded coherent in γ phase. The γ′ phase of the alloy all has a size of about 300-500 nm and a volume content of more than sixty percent. The dimension of γ′ precipitates is reduced and uni?form with increase of Ru content. Ru element can reduce the distribution ratio of high melting point element, so the microstructural stability is enhanced with Ru content increasing. No topologically close-packed (TCP) phase precipitated in the 5% Ru alloy even after 1000 h exposure. The creep rupture life of the alloy is significantly improved as Ru content rising. The raft breadth decreases slightly as Ru content increases. The specimen with 1% Ru and 3% Ru exhibits the presence of TCP phases and without TCP phases precipitated in fracture specimen with 5% Ru. The density and integrity of γ/γ′ interfacial dislocation network increase as Ru content of the alloy rises. |
| Key words: DD15 alloy Ru element stress rupture life microstructure stability |
| DOI：10.11916/j.issn.1005-9113.22061 |
| Clc Number:TG132.3+2 |
| Fund: |
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| Descriptions in Chinese: |
| A fourth generation single crystal (SC) nickel based cast superalloy DD15 with 1%Ru, 3%Ru, 5%Ru was prepared using vacuum induction single crystal furnace in order to optimize the properties and cost of DD15 alloy. The exposure experiment of three alloys was conducted at 1100 ℃ for 1000 h. The stress rupture properties tests were performed at 1100 ℃ temperature and 137 MPa pressure. The composition optimization of Ru element in DD15 alloy had been studied. It was found that the alloys with different Ru contents all consist of cuboidal γ′ phase embedded coherent in γ phase. The γ′ phase of the alloy all has a size of about 300-500 nm and a volume content of more than sixty percent. The dimension of γ′ precipitates is reduced and uni?form with increase of Ru content. Ru element can reduce the distribution ratio of high melting point element, so the microstructural stability is enhanced with Ru content increasing. No topologically close-packed (TCP) phase precipitated in the 5% Ru alloy even after 1000 h exposure. The creep rupture life of the alloy is significantly improved as Ru content rising. The raft breadth decreases slightly as Ru content increases. The specimen with 1% Ru and 3% Ru exhibits the presence of TCP phases and without TCP phases precipitated in fracture specimen with 5% Ru. The density and integrity of γ/γ′ interfacial dislocation network increase as Ru content of the alloy rises. |
